顺酐厂家为大家讲解鉴别顺酐和顺酸的方法:
The maleic anhydride manufacturer will explain the method of identifying maleic anhydride and maleic acid:
1、称取大约相同的量,用水溶解后,再用碱滴定,消耗碱多的是酐,消耗碱少的是酸。
1. Weigh about the same amount, dissolve it with water, and then titrate it with alkali. Anhydride consumes more alkali and acid consumes less alkali.
2、或取少量相同量的样品溶解于水,用pH计检测,pH值低的是酐,pH稍高的是酸。
2. Or take a small amount of the same amount of sample to dissolve in water and test it with a pH meter. The anhydride with low pH value and the acid with slightly higher pH value.
3、用熔点检测也可以,酐与酸的熔点不同。顺酐约52~53℃,顺酸约130℃。
3. It can also be detected by melting point. The melting point of anhydride and acid is different. Maleic anhydride is about 52 ~ 53 ℃, and maleic acid is about 130 ℃.
4、^简单的办法,找一小块不锈钢片,将两种样品各放一点于钢片两侧,用打火机在两个样品中间加热,先液化并挥发的是顺酐。
4. ^ a simple way is to find a small piece of stainless steel sheet, put a little of the two samples on both sides of the steel sheet, and heat them with a lighter. Maleic anhydride is liquefied and volatilized first.